Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete
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Aćimović, Danka D.![](/themes/Mirageriofh/images/orcid.png)
Nikolić, Željka
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Tošić, Miloš
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Milovanović, Dubravka
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Nikolić, Vladimir
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Brdarić, Tanja P.
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Marčeta-Kaninski, Milica
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Human exposure to persistent organic contaminants, from building materials, negatively affects people's health and overall quality of life. This paper presents the validation and uncertainty assessment of the analytical method, developed for the simultaneous determination of 16 EPA polycyclic aromatic hydrocarbons (PAHs) in solid-solid concrete by ultra-performance liquid chromatography with photo diode-array detector. Linearity of calibration curves was good over the whole range of calibration. Limits of detection varied between 0.2 and 2.9 mu gkg(-1). The accuracy in terms of recovery of the validated method is within the range from 54 to 106%. The developed method proved to be appropriate for analysis of PAHs and can be used for the quality control testing of concrete during the construction of new buildings, the old residences and related buildings associated with sick-building syndrome. In addition, this is the first reported method described for the evaluation of PAHs in solid-so...lid concrete.
Keywords:
Validation / UPLC-PDA / Uncertainty / PAH / Concrete / Building materialSource:
Journal of Hazardous Materials, 2017, 325, 271-278Funding / projects:
- Hydrogen Energy - Research and Development of New Materials: Electrolytic Hydrogen Production, Hydrogen Fuel Cells, Isotope Effects (RS-MESTD-Basic Research (BR or ON)-172045)
- Research and verification of the multidisciplinary forensic methods in (RS-MESTD-Technological Development (TD or TR)-37021)
DOI: 10.1016/j.jhazmat.2016.12.008
ISSN: 0304-3894
PubMed: 27940116
WoS: 000392165700027
Scopus: 2-s2.0-85003828415
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Institut za opštu i fizičku hemijuTY - JOUR AU - Aćimović, Danka D. AU - Nikolić, Željka AU - Tošić, Miloš AU - Milovanović, Dubravka AU - Nikolić, Vladimir AU - Brdarić, Tanja P. AU - Marčeta-Kaninski, Milica PY - 2017 UR - https://riofh.iofh.bg.ac.rs/handle/123456789/531 AB - Human exposure to persistent organic contaminants, from building materials, negatively affects people's health and overall quality of life. This paper presents the validation and uncertainty assessment of the analytical method, developed for the simultaneous determination of 16 EPA polycyclic aromatic hydrocarbons (PAHs) in solid-solid concrete by ultra-performance liquid chromatography with photo diode-array detector. Linearity of calibration curves was good over the whole range of calibration. Limits of detection varied between 0.2 and 2.9 mu gkg(-1). The accuracy in terms of recovery of the validated method is within the range from 54 to 106%. The developed method proved to be appropriate for analysis of PAHs and can be used for the quality control testing of concrete during the construction of new buildings, the old residences and related buildings associated with sick-building syndrome. In addition, this is the first reported method described for the evaluation of PAHs in solid-solid concrete. T2 - Journal of Hazardous Materials T1 - Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete EP - 278 SP - 271 VL - 325 DO - 10.1016/j.jhazmat.2016.12.008 UR - conv_642 ER -
@article{ author = "Aćimović, Danka D. and Nikolić, Željka and Tošić, Miloš and Milovanović, Dubravka and Nikolić, Vladimir and Brdarić, Tanja P. and Marčeta-Kaninski, Milica", year = "2017", abstract = "Human exposure to persistent organic contaminants, from building materials, negatively affects people's health and overall quality of life. This paper presents the validation and uncertainty assessment of the analytical method, developed for the simultaneous determination of 16 EPA polycyclic aromatic hydrocarbons (PAHs) in solid-solid concrete by ultra-performance liquid chromatography with photo diode-array detector. Linearity of calibration curves was good over the whole range of calibration. Limits of detection varied between 0.2 and 2.9 mu gkg(-1). The accuracy in terms of recovery of the validated method is within the range from 54 to 106%. The developed method proved to be appropriate for analysis of PAHs and can be used for the quality control testing of concrete during the construction of new buildings, the old residences and related buildings associated with sick-building syndrome. In addition, this is the first reported method described for the evaluation of PAHs in solid-solid concrete.", journal = "Journal of Hazardous Materials", title = "Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete", pages = "278-271", volume = "325", doi = "10.1016/j.jhazmat.2016.12.008", url = "conv_642" }
Aćimović, D. D., Nikolić, Ž., Tošić, M., Milovanović, D., Nikolić, V., Brdarić, T. P.,& Marčeta-Kaninski, M.. (2017). Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete. in Journal of Hazardous Materials, 325, 271-278. https://doi.org/10.1016/j.jhazmat.2016.12.008 conv_642
Aćimović DD, Nikolić Ž, Tošić M, Milovanović D, Nikolić V, Brdarić TP, Marčeta-Kaninski M. Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete. in Journal of Hazardous Materials. 2017;325:271-278. doi:10.1016/j.jhazmat.2016.12.008 conv_642 .
Aćimović, Danka D., Nikolić, Željka, Tošić, Miloš, Milovanović, Dubravka, Nikolić, Vladimir, Brdarić, Tanja P., Marčeta-Kaninski, Milica, "Validation and uncertainty estimation of UPLC-PDA method for the analysis of polycyclic aromatic hydrocarbons in concrete" in Journal of Hazardous Materials, 325 (2017):271-278, https://doi.org/10.1016/j.jhazmat.2016.12.008 ., conv_642 .